Under pressure: offering fundamental insight into structural changes on ...
A second set of ball milling experiments were performed using a Fritsch Pulverisette P23 vibratory ball mill to understand variables of frequency/ball size/time. ... A Bruker mm double channel probe at 50 kHz MAS speed was used with single pulse (d1π/2deACQ) experiment, a s recycle delay (d1), 5 μs prescan delay, ACQ time of 0. ...